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Selection Of The Hplc Method In Chemical Analysis

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Selection of the HPLC Method in Chemical Analysis

Selection of the HPLC Method in Chemical Analysis Book
Author : Serban C. Moldoveanu,Victor David
Publisher : Elsevier
Release : 2016-11-01
ISBN : 0128037113
Language : En, Es, Fr & De

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Book Description :

Selection of the HPLC Method in Chemical Analysis serves as a practical guide to users of high-performance liquid chromatography and provides criteria for method selection, development, and validation. High-performance liquid chromatography (HPLC) is the most common analytical technique currently practiced in chemistry. However, the process of finding the appropriate information for a particular analytical project requires significant effort and pre-existent knowledge in the field. Further, sorting through the wealth of published data and literature takes both time and effort away from the critical aspects of HPLC method selection. For the first time, a systematic approach for sorting through the available information and reviewing critically the up-to-date progress in HPLC for selecting a specific analysis is available in a single book. Selection of the HPLC Method in Chemical Analysis is an inclusive go-to reference for HPLC method selection, development, and validation. Addresses the various aspects of practice and instrumentation needed to obtain reliable HPLC analysis results Leads researchers to the best choice of an HPLC method from the overabundance of information existent in the field Provides criteria for HPLC method selection, development, and validation Authored by world-renowned HPLC experts who have more than 60 years of combined experience in the field

Selection of the HPLC Method in Chemical Analysis

Selection of the HPLC Method in Chemical Analysis Book
Author : Serban C. Moldoveanu,Victor David
Publisher : Elsevier
Release : 2016-11-25
ISBN : 9780128036846
Language : En, Es, Fr & De

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Book Description :

Selection of the HPLC Method in Chemical Analysis serves as a practical guide to users of high performance liquid chromatography, providing exacting criteria for method selection, development, and validation. High performance liquid chromatography is the most common analytical technique currently practiced in chemistry. However, the process of finding the appropriate information for a particular analytical project requires significant effort and pre-existent knowledge in the field. Further, sorting through the wealth of published data and literature takes both time and effort away from the critical aspects of HPLC method selection. This book, for the first time, presents a systematic approach for sorting through the available information, also providing a critical analysis of the progress in HPLC for selecting a specific analysis. It is an inclusive, go-to reference for HPLC method selection, development, and validation. Addresses the various aspects of practice and instrumentation needed to obtain reliable HPLC analysis results Leads researchers to the best choice of an HPLC method from the overabundance of information existing in the field Provides exacting criteria for HPLC method selection, development, and validation Authored by world-renowned HPLC experts who have more than 60 years of combined experience in the field

Biochemical Analysis Tools

Biochemical Analysis Tools Book
Author : Oana-Maria Boldura,Cornel Balta,Prof Nasser Awwad
Publisher : BoD – Books on Demand
Release : 2020-06-24
ISBN : 1789848563
Language : En, Es, Fr & De

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Book Description :

This book explores the role of nucleic acid analysis and the advances it has led to in the field of life sciences. The first section is a collection of chapters covering experimental methods used in molecular biology, the techniques adjacent to these methods, and the steps of analysis before and after obtaining raw DNA data. The second section deals with the principles of chromatography, method development, sample preparation, and industrial applications.

Essentials in Modern HPLC Separations

Essentials in Modern HPLC Separations Book
Author : Serban C. Moldoveanu,Victor David
Publisher : Elsevier
Release : 2022-06-24
ISBN : 0323998364
Language : En, Es, Fr & De

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Book Description :

Essentials in Modern HPLC Separations, Second Edition discusses the role of separation in high performance liquid chromatography (HPLC). This new and updated edition systematically presents basic concepts as well as new developments in HPLC. Starting with a description of basic concepts, it provides important guidance for the practical utilization of various HPLC procedures, such as the selection of the HPLC type, proper choice of the chromatographic column, selection of mobile phase and selection of the method of detection, all of which are in correlation with the physico-chemical characteristics of the compounds separated. Every chapter has been carefully reviewed, with several new sections added to bring the book completely up-to-date. Hence, it is a valuable reference for students and professors in chemistry. Provides a thoroughly updated resource, with an entirely new section on Computer-aided Method Development in HPLC and new subsections on miniaturization and automation in HPLC, chemometric aspects of HPLC, green solvent use in HPLC, and more Includes insights into the chromatographic process to find the optimum solution for analyzing complex samples Presents a basis for understanding the utilization of modern HPLC for applications, particularly for the analysis of pharmaceutical, biological, food, beverage and environmental samples

Intelligent Software for Chemical Analysis

Intelligent Software for Chemical Analysis Book
Author : L.M.C. Buydens,P.J. Schoenmakers
Publisher : Elsevier
Release : 1993-09-03
ISBN : 9780080868400
Language : En, Es, Fr & De

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Book Description :

Various emerging techniques for automating intelligent functions in the laboratory are described in this book. Explanations on how systems work are given and possible application areas are suggested. The main part of the book is devoted to providing data which will enable the reader to develop and test his own systems. The emphasis is on expert systems; however, promising developments such as self-adaptive systems, neural networks and genetic algorithms are also described. The book has been written by chemists with a great deal of practical experience in developing and testing intelligent software, and therefore offers first-hand knowledge. Laboratory staff and managers confronted with commercial intelligent software will find information on the functioning, possibilities and limitations thereof, enabling them to select and use modern software in an optimum fashion. Finally, computer scientists and information scientists will find a wealth of data on the application of contemporary artificial intelligence techniques.

Optimization in HPLC

Optimization in HPLC Book
Author : Stavros Kromidas
Publisher : John Wiley & Sons
Release : 2021-08-06
ISBN : 3527828516
Language : En, Es, Fr & De

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Book Description :

Learn to maximize the performance of your HPLC or UHPLC system with this resource from leading experts in the field Optimization in HPLC: Concepts and Strategies delivers tried-and-tested strategies for optimizing the performance of HPLC and UHPLC systems for a wide variety of analytical tasks. The book explains how to optimize the different HPLC operation modes for a range of analyses, including small molecules, chiral substances, and biomolecules. It also shows readers when and how computational tools may be used to optimize performance. The practice-oriented text describes common challenges faced by users and developers of HPLC and UHPLC systems, as well as how those challenges can be overcome. Written for first-time and experienced users of HPLC technology and keeping pace with recent developments in HPLC instrumentation and operation modes, this comprehensive guide leaves few questions unanswered. Readers will also benefit from the inclusion of: A thorough introduction to optimization strategies for different modes and uses of HPLC, including working under regulatory constraints An exploration of computer aided HPLC optimization, including ChromSwordAuto and Fusion QbD A treatment of current challenges for HPLC users in industry as well as large and small analytical service providers Discussions of current challenges for HPLC equipment suppliers Tailor-made for analytical chemists, chromatographers, pharmacologists, toxicologists, and lab technicians, Optimization in HPLC: Concepts and Strategies will also earn a place on the shelves of analytical laboratories in academia and industry who seek a one-stop reference for optimizing the performance of HPLC systems.

Instrumental Methods of Chemical Analysis

Instrumental Methods of Chemical Analysis Book
Author : Dr. B. K. Sharma
Publisher : Krishna Prakashan Media
Release : 1981
ISBN : 9788182830196
Language : En, Es, Fr & De

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Book Description :

Download Instrumental Methods of Chemical Analysis book written by Dr. B. K. Sharma, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

Chemical Analysis

Chemical Analysis Book
Author : Francis Rouessac,Annick Rouessac
Publisher : John Wiley & Sons
Release : 2022-04-12
ISBN : 1119701333
Language : En, Es, Fr & De

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Book Description :

The new edition of the popular introductory analytical chemistry textbook, providing students with a solid foundation in all the major instrumental analysis techniques currently in use The third edition of Chemical Analysis: Modern Instrumentation Methods and Techniques provides an up-to-date overview of the common methods used for qualitative, quantitative, and structural chemical analysis. Assuming no background knowledge in the subject, this student-friendly textbook covers the fundamental principles and practical aspects of more than 20 separation and spectroscopic methods, as well as other important techniques such as elemental analysis, electrochemistry and isotopic labelling methods. Avoiding technical complexity and theoretical depth, clear and accessible chapters explain the basic concepts of each method and its corresponding instrumental techniques—supported by explanatory diagrams, illustrations, and photographs of commercial instruments. The new edition includes revised coverage of recent developments in supercritical fluid chromatography, capillary electrophoresis, miniaturized sensors, automatic analyzers, digitization and computing power, and more. Offering a well-balanced introduction to a wide range of analytical and instrumentation techniques, this textbook: Provides a detailed overview of analysis methods used in the chemical and agri-food industries, medical analysis laboratories, and environmental sciences Covers various separation methods including chromatography, electrophoresis and electrochromatography Describes UV and infrared spectroscopy, fluorimetry and chemiluminescence, x-ray fluorescence, nuclear magnetic resonance and other common spectrometric methods such atomic or flame emission, atomic absorption and mass spectrometry Includes concise overview chapters on the general aspects of chromatography, sample preparation strategies, and basic statistical parameters Features examples, end-of-chapter problems with solutions, and a companion website featuring PowerPoint slides for instructors Chemical Analysis: Modern Instrumentation Methods and Techniques, Third Edition, is the perfect textbook for undergraduates taking introductory courses in instrumental analytical chemistry, students in chemistry, pharmacy, biochemistry, and environmental science programs looking for information on the techniques and instruments available, and industry technicians working with problems of chemical analysis. Review of Second Edition: “An essential introduction to a wide range of analytical and instrumentation techniques that have been developed and improved in recent years.” --International Journal of Environmental and Analytical Chemistry

HPLC Method Development for Pharmaceuticals

HPLC Method Development for Pharmaceuticals Book
Author : Satinder Ahuja,Henrik Rasmussen
Publisher : Elsevier
Release : 2011-09-21
ISBN : 0080554199
Language : En, Es, Fr & De

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Book Description :

High pressure, or high performance, liquid chromatography (HPLC) is the method of choice for checking purity of new drug candidates, monitoring changes during scale up or revision of synthetic procedures, evaluating new formulations, and running control/assurance of the final drug product. HPLC Method Development for Pharmaceuticals provides an extensive overview of modern HPLC method development that addresses these unique concerns. Includes a review and update of the current state of the art and science of HPLC, including theory, modes of HPLC, column chemistry, retention mechanisms, chiral separations, modern instrumentation (including ultrahigh-pressure systems), and sample preparation. Emphasis has been placed on implementation in a pharmaceutical setting and on providing a practical perspective. HPLC Method Development for Pharmaceuticals is intended to be particularly useful for both novice and experienced HPLC method development chemists in the pharmaceutical industry and for managers who are seeking to update their knowledge. Covers the requirements for HPLC in a pharmaceutical setting including strategies for software and hardware validation to allow for use in a regulated laboratory Provides an overview of the pharmaceutical development process (clinical phases, chemical and pharmaceutical development activities) Discusses how HPLC is used in each phase of pharmaceutical development and how methods are developed to support activities in each phase

Amino Acids Peptides and Proteins in Organic Chemistry Analysis and Function of Amino Acids and Peptides

Amino Acids  Peptides and Proteins in Organic Chemistry  Analysis and Function of Amino Acids and Peptides Book
Author : Anonim
Publisher : John Wiley & Sons
Release : 2013-02-13
ISBN : 3527631852
Language : En, Es, Fr & De

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Book Description :

This is the last of five books in the Amino Acids, Peptidesand Proteins in Organic Synthesis series. Closing a gap in the literature, this is the only series tocover this important topic in organic and biochemistry. Drawingupon the combined expertise of the international "who's who" inamino acid research, these volumes represent a real benchmark foramino acid chemistry, providing a comprehensive discussion of theoccurrence, uses and applications of amino acids and, by extension,their polymeric forms, peptides and proteins. The practical value of each volume is heightened by theinclusion of experimental procedures. The 5 volumes cover the following topics: Volume 1: Origins and Synthesis of Amino Acids Volume 2: Modified Amino Acids, Organocatalysis and Enzymes Volume 3: Building Blocks, Catalysis and Coupling Chemistry Volume 4: Protection Reactions, Medicinal Chemistry,Combinatorial Synthesis Volume 5: Analysis and Function of Amino Acids and Peptides Volume 5 of this series presents a wealth of methods to analyzeamino acids and peptides. Classical approaches are described, suchas X-ray analysis, chromatographic methods, NMR, AFM, massspectrometry and 2D-gel electrophoresis, as well as newerapproaches, including Surface Plasmon Resonance and arraytechnologies. Originally planned as a six volume series, Amino Acids,Peptides and Proteins in Organic Chemistry now completes withfive volumes but remains comprehensive in both scope andcoverage. ahref="http://eu.wiley.com/WileyCDA/WileyTitle/productCd-3527335463.html"Furtherinformation about the 5 Volume Set and purchasing details can beviewed here./a

Ionic Liquids in Catalysis

Ionic Liquids in Catalysis Book
Author : Hieronim Maciejewski
Publisher : MDPI
Release : 2021-08-30
ISBN : 3036512462
Language : En, Es, Fr & De

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Book Description :

Due to their distinctive properties, ionic liquids have attracted the great and unflagging interest of researchers for over 30 years. This interest has been focused mainly on their use as a green alternative to volatile organic solvents. However, they often act not only as solvents but also as catalysts, catalyst immobilizers and initiators. Over 100 types of chemical reactions are known in which ionic liquids (ILs) were applied successfully. This Special Issue is aimed at showing the most recent advances and trends in the design, synthesis and characterization of catalysts based on ILs, as well as presenting their activity and application potential.

Analytical Chemistry

Analytical Chemistry Book
Author : Harold H. Trimm
Publisher : CRC Press
Release : 2011-04-15
ISBN : 1926692586
Language : En, Es, Fr & De

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Book Description :

This collection presents a broad selection of recent research on analytical chemistry, including methods of determination and analysis as applied to plants, pharmaceuticals, foods, proteins, and more. Analytical chemistry is the study of what chemicals are present and in what amount in natural and artificial materials. Because these understandings are fundamental in just about every chemical inquiry, analytical chemistry is used to obtain information, ensure safety, and solve problems in many different chemical areas, and is essential in both theoretical and applied chemistry. Analytical chemistry is driven by new and improved instrumentation.

Calibration and Validation of Analytical Methods

Calibration and Validation of Analytical Methods Book
Author : Mark Stauffer
Publisher : BoD – Books on Demand
Release : 2018-04-25
ISBN : 1789230845
Language : En, Es, Fr & De

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Book Description :

This book seeks to introduce the reader to current methodologies in analytical calibration and validation. This collection of contributed research articles and reviews addresses current developments in the calibration of analytical methods and techniques and their subsequent validation. Section 1, "Introduction," contains the Introductory Chapter, a broad overview of analytical calibration and validation, and a brief synopsis of the following chapters. Section 2 "Calibration Approaches" presents five chapters covering calibration schemes for some modern analytical methods and techniques. The last chapter in this section provides a segue into Section 3, "Validation Approaches," which contains two chapters on validation procedures and parameters. This book is a valuable source of scientific information for anyone interested in analytical calibration and validation.

Introduction to Pharmaceutical Chemical Analysis

Introduction to Pharmaceutical Chemical Analysis Book
Author : Steen Hansen,Steen Honoré Hansen,Stig Pedersen-Bjergaard,Knut Rasmussen
Publisher : John Wiley & Sons
Release : 2011-12-12
ISBN : 0470661224
Language : En, Es, Fr & De

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Book Description :

This textbook is the first to present a systematic introduction to chemical analysis of pharmaceutical raw materials, finished pharmaceutical products, and of drugs in biological fluids, which are carried out in pharmaceutical laboratories worldwide. In addition, this textbook teaches the fundamentals of all the major analytical techniques used in the pharmaceutical laboratory, and teaches the international pharmacopoeias and guidelines of importance for the field. It is primarily intended for the pharmacy student, to teach the requirements in “analytical chemistry” for the 5 years pharmacy curriculum, but the textbook is also intended for analytical chemists moving into the field of pharmaceutical analysis. Addresses the basic concepts, then establishes the foundations for the common analytical methods that are currently used in the quantitative and qualitative chemical analysis of pharmaceutical drugs Provides an understanding of common analytical techniques used in all areas of pharmaceutical development Suitable for a foundation course in chemical and pharmaceutical sciences Aimed at undergraduate students of degrees in Pharmaceutical Science/Chemistry Analytical Science/Chemistry, Forensic analysis Includes many illustrative examples

Nanomaterials in Bionanotechnology

Nanomaterials in Bionanotechnology Book
Author : Ravindra Pratap Singh,Kshitij RB Singh
Publisher : CRC Press
Release : 2021-08-18
ISBN : 1000428346
Language : En, Es, Fr & De

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Book Description :

Nanomaterials in Bionanotechnology: Fundamentals and Applications offers a comprehensive treatment of nanomaterials in biotechnology from fundamentals to applications, along with their prospects. This book explains the basics of nanomaterial properties, synthesis, biological synthesis, and chemistry and demonstrates how to use nanomaterials to overcome problems in agricultural, environmental, and biomedical applications. Features Covers nanomaterials for environmental analysis and monitoring for heavy metals, chemical toxins, and water pollutant detection Describes nanomaterials-based biosensors and instrumentation and use in disease diagnosis and therapeutics Discusses nanomaterials for food processing and packaging and agricultural waste management Identifies challenges in nanomaterials-based technology and how to solve them This work serves as a reference for industry professionals, advanced students, and researchers working in the discipline of bionanotechnology.

Computer assisted Method Development for High performance Liquid Chromatography

Computer assisted Method Development for High performance Liquid Chromatography Book
Author : Joseph L. Glajch,Lloyd R. Snyder
Publisher : Elsevier Science Limited
Release : 1990
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

This book deals with the use of the computer as an aid in selecting adequate or optimum conditions for a given analytical separation. Originally published as Volume 485 of the Journal of Chromatography, it has now been reprinted in book form, since the information is so useful that many chromatographers want a copy readily available in the lab. An extensive Introduction is added to the book edition. This surveys the field and refers to the pages where particular items are discussed in the book. The addition of a Glossary of Terms, an Author Index and a Subject Index make this book an invaluable source of easily consulted information for the practising chromatographer. For the purpose of this book, computer-assisted method development will be limited to specific procedures which are intended to be used with a computer - rather than their manually applied precursors. In that sense, the subject can be considered to have begun around 1980. The ongoing, intense research activity into various forms of computer assisted HPLC method development provides the assurance that this approach can really assist the practical chromatographer working in an industrial laboratory.

Selected Water Resources Abstracts

Selected Water Resources Abstracts Book
Author : Anonim
Publisher : Unknown
Release : 1991
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download Selected Water Resources Abstracts book written by , available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

Practical HPLC Method Development

Practical HPLC Method Development Book
Author : Lloyd R. Snyder,Joseph J. Kirkland,Joseph L. Glajch
Publisher : John Wiley & Sons
Release : 2012-12-03
ISBN : 1118591518
Language : En, Es, Fr & De

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Book Description :

This revision brings the reader completely up to date on the evolving methods associated with increasingly more complex sample types analyzed using high-performance liquid chromatography, or HPLC. The book also incorporates updated discussions of many of the fundamental components of HPLC systems and practical issues associated with the use of this analytical method. This edition includes new or expanded treatments of sample preparation, computer assisted method development, as well as biochemical samples, and chiral separations.

Handbook of Analytical Validation

Handbook of Analytical Validation Book
Author : Michael E. Swartz,Ira S. Krull
Publisher : CRC Press
Release : 2012-04-24
ISBN : 142001448X
Language : En, Es, Fr & De

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Book Description :

Written for practitioners in both the drug and biotechnology industries, the Handbook of Analytical Validation carefully compiles current regulatory requirements on the validation of new or modified analytical methods. Shedding light on method validation from a practical standpoint, the handbook:Contains practical, up-to-date guidelines for analyti

Guidance for the Validation of Analytical Methodology and Calibration of Equipment Used for Testing of Illicit Drugs in Seized Materials and Biological Specimens

Guidance for the Validation of Analytical Methodology and Calibration of Equipment Used for Testing of Illicit Drugs in Seized Materials and Biological Specimens Book
Author : United Nations
Publisher : United Nations Publications
Release : 2009
ISBN : 9789211482430
Language : En, Es, Fr & De

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Book Description :

The validation of analytical methods and the calibration of equipment are important aspects of quality assurance in the laboratory. This manual deals with both of these within the context of testing of illicit drugs in seized materials and biological specimens. It provides an introduction and practical guidance to national authorities and analysts in the implementation of method validation and verification, and also in the calibration/performance verification of laboratory instrumentation and equipment within their existing internal quality assurance programmes. The procedures described represent a synthesis of the experience of scientists from several reputable laboratories around the world.