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Microwaves In Chemistry Applications

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Microwaves in Chemistry Applications

Microwaves in Chemistry Applications Book
Author : Bimal K. Banik,Aparna Das
Publisher : Elsevier
Release : 2021-05-01
ISBN : 0128230851
Language : En, Es, Fr & De

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Book Description :

Microwaves in Chemistry Applications: Fundamentals, Methods and Future Trends offers a number of benefits over conventional heating technologies, including acceleration of reaction rates, milder reaction conditions, higher chemical yields, lower energy usage and different reaction selectivity, all of which can improve the sustainability of processes. The book provides valuable insights into the underlying chemistry at play in microwave-assisted processes, introducing fundamental concepts, discussing the modeling of reactions in such processes, and also highlighting a range of key methods and applications of microwaves in chemistry for improved sustainability. Beginning with an introduction to microwave chemistry, Part One discusses foundational principles, equipment and approaches for modeling reactions and assessing the outputs of those models. Methods in microwave chemistry are then the focus of Part Two, with microwave-assisted synthesis, catalysis, reduction and reactions all explored in detail. Part Three reflects on the practical usage of these methods to address specific issues, covering a number of interesting applications. Provides guidance on the modeling and interpretation of microwave effects Discusses microwave chemistry in the context of green chemistry principles Outlines a range of important microwave methods, including microwave-assisted synthesis, catalysis, reactions and reductions

Microwave Synthesis

Microwave Synthesis Book
Author : Brittany L. Hayes
Publisher : Cem Corporation
Release : 2002
ISBN :
Language : En, Es, Fr & De

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Book Description :

1. Introduction to microwave chemistry 11; 2. Solvents 29; 3. Chemical reactions in the presence and absence of solvent 77; 4. Synthetic applications 95; 5. Getting started with microwave synthesis 157; 6. Microwave safety considerations 175; 7. Microwave hardware 181.

Microwaves in Nanoparticle Synthesis

Microwaves in Nanoparticle Synthesis Book
Author : Satoshi Horikoshi,Nick Serpone
Publisher : John Wiley & Sons
Release : 2013-05-03
ISBN : 3527648143
Language : En, Es, Fr & De

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Book Description :

For the first time, this comprehensive handbook presents the emerging field of microwave technology for the synthesis of nanoparticles. Divided into three parts--fundamentals, methods, and applications--it covers topics including microwave theory, scale-up, microwave plasma synthesis, characterization, and more. This offers both an important volume for academic researchers, and a resource for those in industry exploring the applications of nanoparticles in semiconductors, electronics, catalysis, sensors, and more.

Advances in Microwave Chemistry

Advances in Microwave Chemistry Book
Author : Bimal K Banik,Debasish Bandyopadhyay
Publisher : CRC Press
Release : 2018-12-07
ISBN : 1351240471
Language : En, Es, Fr & De

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Book Description :

Advances in Microwave Chemistry discusses the novel bond formation methodologies, synergistic effects of microwaves with other entities, sample preparation including digestion, combustion, and extraction techniques, as well as selectivity in chemical processes. Recent updates are provided on microwave-assisted syntheses of pharmacologically significant aza-, oxo- and other heterocycles, including lactams, nucleosides, bile acids and sterols, the preparation of nanomaterials, composites, and absorber layer materials for thin film. This book also incorporates comparative discussions involving microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry. Key Features: Provides a comparative discussion on microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry Presents recent applications of microwave radiation in biocatalysis Offers a complete package correlating various aspects of microwaves in organic syntheses, the biological impact of products formed in reactions, pharmacological features, and environmental sustainability of the procedures Explains microwave-induced reactions on structurally complex bile acids and sterols Stands as a valuable and unique addition to the well-established book series, New Directions in Organic and Biological Chemistry

Microwaves in Catalysis

Microwaves in Catalysis Book
Author : Satoshi Horikoshi,Nick Serpone
Publisher : John Wiley & Sons
Release : 2015-12-14
ISBN : 3527338152
Language : En, Es, Fr & De

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Book Description :

A comprehensive overview covering the principles and preparation of catalysts, as well as reactor technology and applications in the field of organic synthesis, energy production, and environmental catalysis. Edited and authored by renowned and experienced scientists, this reference focuses on successful reaction procedures for applications in industry. Topics include catalyst preparation, the treatment of waste water and air, biomass and waste valorisation, hydrogen production, oil refining as well as organic synthesis in the presence of heterogeneous and homogeneous catalysts and continuous-flow reactions. With its practical relevance and successful methodologies, this is a valuable guide for chemists at universities working in the field of catalysis, organic synthesis, pharmaceutical or green chemistry, as well as researchers and engineers in the chemical industry.

Microwaves in Organic and Medicinal Chemistry

Microwaves in Organic and Medicinal Chemistry Book
Author : C. Oliver Kappe,Alexander Stadler
Publisher : John Wiley & Sons
Release : 2006-05-12
ISBN : 3527606831
Language : En, Es, Fr & De

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Book Description :

The authors of this guide are experts on the use of microwaves for drug synthesis as well as having much experience in teaching courses held under the auspices of the American Chemical Society and the IUPAC. In this handy source of information for any practicing synthetic chemist they focus on common reaction types in medicinal chemistry, including solid-phase and combinatorial methods. They consider the underlying theory, latest developments in microwave applications and include a variety of examples from recent literature, as well as less common applications that are equally relevant for organic and medicinal chemists. An indispensable reference for researchers with an affinity to modern methods.

Microwaves in Organic Synthesis

Microwaves in Organic Synthesis Book
Author : Antonio de la Hoz,André Loupy
Publisher : John Wiley & Sons
Release : 2013-02-26
ISBN : 3527651330
Language : En, Es, Fr & De

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Book Description :

The third edition of the bestselling two-volume reference covers everything you need to know about microwave technology for synthesis - from the best equipment to nonthermal effects, from solid-support reactions to catalysis. Completely revised and updated with half of the authors completely new to the project, this comprehensive work is clearly divided into two parts on the fundamentals of microwave irradiation, and application of microwaves and synergies with other enabling techniques. Also new to this edition are chapters on on-line monitoring, flow chemistry, combination with ultrasounds and natural products, including multicomponent reactions. An indispensable source for organic, catalytic, physical, and medicinal chemists.

Handbook of Microwave Technology for Food Application

Handbook of Microwave Technology for Food Application Book
Author : Ashim K. Datta
Publisher : CRC Press
Release : 2001-04-27
ISBN : 9780824704902
Language : En, Es, Fr & De

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Book Description :

"Integrates principles of electromagnetics, dielectrics, heat and moisture transfer, packaging, solid mechanics, fluid flow, food chemistry, and microbiology to provide a comprehensive overview of microwave processing in a single accessible source."

Microwave Chemistry

Microwave Chemistry Book
Author : Giancarlo Cravotto,Diego Carnaroglio
Publisher : Walter de Gruyter GmbH & Co KG
Release : 2017-09-25
ISBN : 3110479931
Language : En, Es, Fr & De

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Book Description :

Microwave Chemistry has changed the way to work in chemical laboratories and is an established state-of-the-art technology to accelarate and enhance chemical processes. This book not only gives an overview of the technology, its historical development and theoretical background, but also presents its exceptionally broad spectrum of applications. Microwave Chemistry enables graduate students and scientist to learn and apply its methods successfully.

Microwave Chemical and Materials Processing

Microwave Chemical and Materials Processing Book
Author : Satoshi Horikoshi,Robert F. Schiffmann,Jun Fukushima,Nick Serpone
Publisher : Springer
Release : 2017-11-28
ISBN : 9811064660
Language : En, Es, Fr & De

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Book Description :

The principal aim of this book is to introduce chemists through a tutorial approach to the use of microwaves by examining several experiments of microwave chemistry and materials processing. It will subsequently enable chemists to fashion their own experiments in microwave chemistry or materials processing. Microwave heating has become a popular methodology in introducing thermal energy in chemical reactions and material processing in laboratory-scale experiments. Several research cases where microwave heating has been used in a wide range of fields have been reported, including organic synthesis, polymers, nanomaterials, biomaterials, and ceramic sintering, among others. In most cases, microwave equipment is used as a simple heat source. Therefore the principal benefits of microwave radiation have seldom been taken advantage of. One reason is the necessity to understand the nature of electromagnetism, microwave engineering, and thermodynamics. However, it is difficult for a chemist to appreciate these in a short time, so they act as barriers for the chemist who might take an interest in the use of microwave radiation. This book helps to overcome these barriers by using figures and diagrams instead of equations as much as possible.

Sustainable Flow Chemistry

Sustainable Flow Chemistry Book
Author : Luigi Vaccaro
Publisher : John Wiley & Sons
Release : 2017-03-14
ISBN : 3527689087
Language : En, Es, Fr & De

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Book Description :

This ready reference not only presents the hot and emerging topic of modern flow chemistry, it is also unique in illustrating the important connection to sustainable chemistry. Focusing on more sustainable methods and applications, the text extensively covers every important field from reaction time optimization to waste minimization, and from safety improvements to microwave applications. In addition, green metrics are presented as a key aspect of the book, helping readers to evaluate the efficiency of flow technologies and their impact on the overall efficiency of a chemical process. An invaluable handbook for every chemist working in the laboratory, whether in academia or industry.

Solid State Chemistry and its Applications

Solid State Chemistry and its Applications Book
Author : Anthony R. West
Publisher : John Wiley & Sons
Release : 2014-01-08
ISBN : 1118676254
Language : En, Es, Fr & De

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Book Description :

Solid State Chemistry and its Applications, 2nd Edition: Student Edition is an extensive update and sequel to the bestselling textbook Basic Solid State Chemistry, the classic text for undergraduate teaching in solid state chemistry worldwide. Solid state chemistry lies at the heart of many significant scientific advances from recent decades, including the discovery of high-temperature superconductors, new forms of carbon and countless other developments in the synthesis, characterisation and applications of inorganic materials. Looking forward, solid state chemistry will be crucial for the development of new functional materials in areas such as energy, catalysis and electronic materials. This revised edition of Basic Solid State Chemistry has been completely rewritten and expanded to present an up-to-date account of the essential topics and recent developments in this exciting field of inorganic chemistry. Each section commences with a gentle introduction, covering basic principles, progressing seamlessly to a more advanced level in order to present a comprehensive overview of the subject. This new Student Edition includes the following updates and new features: Expanded coverage of bonding in solids, including a new section on covalent bonding and more extensive treatment of metallic bonding. Synthetic methods are covered extensively and new topics include microwave synthesis, combinatorial synthesis, mechano-synthesis, atomic layer deposition and spray pyrolysis. Revised coverage of electrical, magnetic and optical properties, with additional material on semiconductors, giant and colossal magnetoresistance, multiferroics, LEDs, fibre optics and solar cells, lasers, graphene and quasicrystals. Extended chapters on crystal defects and characterisation techniques. Published in full colour to aid comprehension. Extensive coverage of crystal structures for important families of inorganic solids is complemented by access to CrystalMaker® visualization software, allowing readers to view and rotate over 100 crystal structures in three dimensions. Solutions to exercises and supplementary lecture material are available online. Solid State Chemistry and its Applications, 2nd Edition: Student Edition is a must-have textbook for any undergraduate or new research worker studying solid state chemistry.

Microwave Assisted Sample Preparation for Trace Element Determination

Microwave Assisted Sample Preparation for Trace Element Determination Book
Author : Erico Marlon Moraes Flores
Publisher : Newnes
Release : 2014-05-03
ISBN : 0444594442
Language : En, Es, Fr & De

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Book Description :

Microwave-Assisted Sample Preparation for Trace Element Analysis describes the principles, equipment, and applications involved in sample preparation with microwaves for trace element analysis. The book covers well-established applications as well as new trends in this field. Hot topics such as sample preparation for speciation, metabolomics, and halogen determination, as well as the alternatives of sample preparation for special samples (for example, carbon nanotubes, polymers, petroleum products), are also discussed. The use of microwaves in sample preparation has increased in recent decades. Several applications of microwaves for sample preparation can be found in the literature for practically all types of sample matrices, especially for the determination of trace elements by atomic spectrometric techniques, safely and cleanly reducing the time involved in this step. Microwave-assisted sample preparation is not only a tool for research but also for routine analysis laboratories; the state-of-the-art in sample preparation in trace element analysis. This book is the only resource for chemists specifically focused on this topic. The first book to describe the principles, equipment, and applications in microwave-assisted sample preparation Written by experts in the field who provide a comprehensive overview of the important concepts Introduces new alternatives and trends in microwave-assisted techniques

Microwave Engineering of Nanomaterials

Microwave Engineering of Nanomaterials Book
Author : Erwann Guenin
Publisher : CRC Press
Release : 2016-03-30
ISBN : 9814669431
Language : En, Es, Fr & De

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Book Description :

The use of microwaves has gradually democratized itself in several scientific areas and is now a common methodology in domains as different as chemistry, protein digestion, mining, and metallurgy. Materials chemistry is one field where microwave irradiation technologies are being studied. In recent years, development of nanotechnologies has increased the interest of materials scientists in these new technologies. Microwave methodologies are now routinely used in several areas of materials science, and new advances are ongoing. This book presents recent improvements in microwave engineering of materials and nanomaterials, interactions of microwave chemistry with materials, and advances in microwave technologies in several domains such as polymer synthesis and modification, processing of various materials (ceramics, glasses, metallic alloys, zeolites), and synthesis and functionalization of diverse nanomaterials (carbon nanotubes, MOF semiconductors, inorganic nanoparticles). The book will be of interest to all students and researchers in materials science and nanosciences who want to discover or increase their knowledge of microwave technology.

Microwave Processing of Materials

Microwave Processing of Materials Book
Author : National Research Council,Division on Engineering and Physical Sciences,National Materials Advisory Board,Commission on Engineering and Technical Systems,Committee on Microwave Processing of Materials: An Emerging Industrial Technology
Publisher : National Academies Press
Release : 1994-02-01
ISBN : 0309050278
Language : En, Es, Fr & De

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Book Description :

Microwaves can be effectively used in the processing of industrial materials under a wide range of conditions. However, microwave processing is complex and multidisciplinary in nature, and a high degree of technical knowledge is needed to determine how, when, and where the technology can be most profitably utilized. This book assesses the potential of microwave technology for industrial applications, reviews the latest equipment and processing methods, and identifies both the gaps in understanding of microwave processing technology and the promising development opportunities that take advantage of this new technology's unique performance characteristics.

Dynamics in Microwave Chemistry

Dynamics in Microwave Chemistry Book
Author : Kama Huang,Xiaoqing Yang,Huacheng Zhu
Publisher : Springer
Release : 2020-12-26
ISBN : 9789811596544
Language : En, Es, Fr & De

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Book Description :

This book addresses microwave chemistry at both the physical and molecular level. Its main goal is to elaborate the highly complex scientific issues involved in the fundamental theory of microwave chemistry, and in industrialized applications in the near future.The book provides detailed insights into the characterization and measurement of dielectric properties under complex conditions, such as chemical reactions, high-temperature environments, etc. Considerable attention is paid to the theory of dynamics in microwave chemistry, from the view of both physical level and molecular level. Microwave-Material Interactions simulation is used for physical dynamical analysis, while a Microwave-Molecules Interactions methodology is proposed for molecular dynamical analysis. In turn, calculational examples are introduced for better description and validation, respectively. Lastly, the book proposes design strategies and calculational examples for large-scale application. Richly illustrated and including a wealth of worked-out examples, this book is ideal for all researchers, students and engineers who are just getting started in the dynamics of microwave chemistry.

Microwave Assisted Proteomics

Microwave Assisted Proteomics Book
Author : Jennie R. Lill
Publisher : Royal Society of Chemistry
Release : 2009-05-15
ISBN : 085404194X
Language : En, Es, Fr & De

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Book Description :

An introduction to the rapidly evolving field of microwave-assisted bio-analytical methods with an emphasis on sample preparation for proteomic analyses.

Microwave Methods in Organic Synthesis

Microwave Methods in Organic Synthesis Book
Author : Prasad Appukkuttan
Publisher : Springer Science & Business Media
Release : 2006-10-09
ISBN : 3540367578
Language : En, Es, Fr & De

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Book Description :

We are delighted to present this volume with contributions from some of the most renowned and experienced microwavechemists today. The delivery and introduction of energy has been closely connected with the discovery and investigation of new chemistry. It is with pleasure that we have seen an increased use of microwave irradiation over the years and we hope that this volume will re?ect the current interest in expanding the scopeofmicrowaveapplicationsinbothorganicandmedicinalchemistry. One important explanation behind the growth of microwave-enhanced chemistry has been the introductionof dedicated microwavereactors. As a result of this development we are proud to present a diverse set of - views. Apart fromchapters spanning the scope that is usually associated with microwavemethods, such as heterocyclic chemistry – an intriguing, but fr- tratingly diverse?eld that is excellently presented in one of the reviews – and transition metal-catalyzed reactions, we also present a review on microwa- assisted natural product chemistry, a topic that is of high interest and neither often nor widely covered. A contribution on microwave-accelerated synt- sis of protease inhibitors underlines the usefulness of microwave heating in medicinal chemistryandareview of?uorousmicrowavechemistryhighlights the importance of the combination of high-speed reactions and quick sepa- tions. Two separate chaptersonscaled-up microwavereactionsandgreen and sustainablechemistrygiveanoverviewofaspectsofmicrowavechemistrythat mightbeofgreatuseinbothindustrialandsmall-scaleapplications. We would like to take this opportunity to express our sincere gratitude to the contributors of this volume for their valuable time and efforts. We believe that the presented workwill further promotethe use of controlledmicrowave heating in both academia and industry.

Microwave enhanced Chemistry

Microwave enhanced Chemistry Book
Author : Howard M. Kingston,Stephen John Haswell
Publisher : Amer Chemical Society
Release : 1997
ISBN :
Language : En, Es, Fr & De

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Book Description :

This book is an indication of the breadth of microwave-enhanced chemistry as a new branch of chemical science. Microwave radiation can be used in many fields of chemistry in addition to sample preparation, decomposition, and extraction. It is now commonly used in the synthesis of organic, organometallic, and inorganic compounds or catalysts.