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Mechanochemical Organic Synthesis

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Mechanochemical Organic Synthesis

Mechanochemical Organic Synthesis Book
Author : Davor Margetic,Vjekoslav Štrukil
Publisher : Elsevier
Release : 2016-04-23
ISBN : 0128025255
Language : En, Es, Fr & De

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Book Description :

Mechanochemical Organic Synthesis is a comprehensive reference that not only synthesizes the current literature but also offers practical protocols that industrial and academic scientists can immediately put to use in their daily work. Increasing interest in green chemistry has led to the development of numerous environmentally-friendly methodologies for the synthesis of organic molecules of interest. Amongst the green methodologies drawing attention, mechanochemistry is emerging as a promising method to circumvent the use of toxic solvents and reagents as well as to increase energy efficiency. The development of synthetic strategies that require less, or the minimal, amount of energy to carry out a specific reaction with optimum productivity is of vital importance for large-scale industrial production. Experimental procedures at room temperature are the mildest reaction conditions (essentially required for many temperature-sensitive organic substrates as a key step in multi-step sequence reactions) and are the core of mechanochemical organic synthesis. This green synthetic method is now emerging in a very progressive manner and until now, there is no book that reviews the recent developments in this area. Features cutting-edge research in the field of mechanochemical organic synthesis for more sustainable reactions Integrates advances in green chemistry research into industrial applications and process development Focuses on designing techniques in organic synthesis directed toward mild reaction conditions Includes global coverage of mechanochemical synthetic protocols for the generation of organic compounds

Mechanochemical Organic Synthesis

Mechanochemical Organic Synthesis Book
Author : Davor Margetic,Vjekoslav Trukil
Publisher : Elsevier
Release : 2016-06-01
ISBN : 9780128021842
Language : En, Es, Fr & De

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Book Description :

Mechanochemical Organic Synthesis is a comprehensive reference that not only synthesizes the current literature but also offers practical protocols that industrial and academic scientists can immediately put to use in their daily work. Increasing interest in green chemistry has led to the development of numerous environmentally-friendly methodologies for the synthesis of organic molecules of interest. Amongst the green methodologies drawing attention, mechanochemistry is emerging as a promising method to circumvent the use of toxic solvents and reagents as well as to increase energy efficiency. The development of synthetic strategies that require less, or the minimal, amount of energy to carry out a specific reaction with optimum productivity is of vital importance for large-scale industrial production. Experimental procedures at room temperature are the mildest reaction conditions (essentially required for many temperature-sensitive organic substrates as a key step in multi-step sequence reactions) and are the core of mechanochemical organic synthesis. This green synthetic method is now emerging in a very progressive manner and until now, there is no book that reviews the recent developments in this area. Features cutting-edge research in the field of mechanochemical organic synthesis for more sustainable reactions Integrates advances in green chemistry research into industrial applications and process development Focuses on designing techniques in organic synthesis directed toward mild reaction conditions Includes global coverage of mechanochemical synthetic protocols for the generation of organic compounds

Exploring Mechanochemistry for Organic Synthesis

Exploring Mechanochemistry for Organic Synthesis Book
Author : Joseph Howard
Publisher : Unknown
Release : 2018
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download Exploring Mechanochemistry for Organic Synthesis book written by Joseph Howard, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

Organic Synthesis

Organic Synthesis Book
Author : Belakatte Parameshwarappa Nandeshwarappa
Publisher : BoD – Books on Demand
Release : 2020-05-27
ISBN : 1789859433
Language : En, Es, Fr & De

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Book Description :

The book ‘Organic Synthesis - A Nascent Relook’ is a compendium of the recent progress in all aspects of organic chemistry including bioorganic chemistry, organo-metallic chemistry, asymmetric synthesis, heterocyclic chemistry, natural product chemistry, catalytic, green chemistry and medicinal chemistry, polymer chemistry, as well as analytical methods in organic chemistry. The book presents the latest developments in these fields. The chapters are written by chosen experts who are internationally known for their eminent research contributions. Organic synthesis is the complete chemical synthesis of a target molecule. In this book, special emphasis is given to the synthesis of various bioactive heterocycles. Careful selection of various topics in this book will serve the rightful purpose for the chemistry community and the industrial houses at all levels.

Ball Milling Towards Green Synthesis

Ball Milling Towards Green Synthesis Book
Author : Brindaban Ranu,Achim Stolle
Publisher : Royal Society of Chemistry
Release : 2014-11-26
ISBN : 1782621989
Language : En, Es, Fr & De

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Book Description :

Ball milling has emerged as a powerful tool over the past few years for effecting chemical reactions by mechanical energy. Allowing a variety of reactions to occur at ambient temperatures and in solvent-free conditions, ball milling presents a greener route for many chemical processes. Compared to the use of microwave and ultrasound as energy sources for chemical reactions, ball milling is not as familiar to chemists and yet it holds great potential. This book will introduce practicing chemists to the technique and will highlight its importance for green transformations. Current applications of ball milling will be covered in detail as well as its origin, recent developments and future scope, challenges and prospects. Chemical transformations covered include carbon-carbon and carbon-heteroatom bond formation, oxidation by solid oxidants, asymmetric organo-catalytic reactions, dehydrogenative coupling, peptide syntheses and polymeric material syntheses. The book will provide a valuable guide for organic, inorganic and organometallic chemists, material scientists, polymer scientists, reaction engineers and postgraduate students in chemistry.

Nontraditional Activation Methods in Green and Sustainable Applications

Nontraditional Activation Methods in Green and Sustainable Applications Book
Author : Bela Torok,Christian Schaefer
Publisher : Elsevier
Release : 2021-02-28
ISBN : 0128190159
Language : En, Es, Fr & De

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Book Description :

Nontraditional Activation Methods in Green and Sustainable Applications: Microwaves; Ultrasounds; Photo-, Electro- and Mechan-ochemistry and High Hydrostatic Pressure provides a broad overview of non-traditional activation methods to help readers identify and use appropriate approaches in reducing the environmental impact of their work. Sections discuss the fundamental principles of each method and provide examples of their practical use, illustrating their usefulness. Given the importance of expanding laboratory based technologies to the industrial level, chapters that cover both existing and potential industrial and environmental applications are also included. Highlighting the usefulness and adaptability of these methods for a range of practical applications, this book is a practical guide for both those involved with the design and application of synthetic methodologies and those interested in the implementation and impact of green chemistry principles in practice, from synthetic and medicinal chemists, to food developers and environmental policy planners. Discusses, and critically assesses, the advantages of non-traditional activation methods in green and sustainable chemistry applications Features individual chapters written by renowned experts in the field Contains extensive, state-of-the-art reference sections, providing critically filtered information to readers

Soft Mechanochemical Synthesis

Soft Mechanochemical Synthesis Book
Author : Evgeniĭ Grigorʹevich Avvakumov,G.V. Avvakumov,Mamoru Senna,N. V. Kosova
Publisher : Springer Science & Business Media
Release : 2001-07-31
ISBN : 0792374312
Language : En, Es, Fr & De

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Book Description :

Mechanical methods of the activation of chemical processes are currently widely used for the synthesis of various compounds. The present monograph deals with the development of a novel approach to mechanochemical synthesis based on reactions of solid acids, bases, hydrated compounds, crystal hydrates, basic and acidic salts. This method has been called soft mechanochemical synthesis. The monograph includes the papers published by the present authors. They describe the results of their investigations n the last two decades. New theoretical and experimental data on kinetics and mechanism of soft mechanochemical reactions in the mixtures of compounds mentioned above to give complex oxide compounds are presented. The description of new high energetic and high efficient mills providing effective occurrence of these reactions is delivered. The possibilities of applying soft mechanochemical synthesis for materials used in catalysts, material science, electronics, etc., are discussed. The advantages of the method proposed in comparison with other methods are demonstrated. The monograph is designed for researchers, engineers and technicians engaged in chemical and ceramic industry, for scientists and students specialized in the area of development, and application of new materials.

Mechanochemical Synthesis of Cocrystals and Metal Organic Materials

Mechanochemical Synthesis of Cocrystals and Metal Organic Materials Book
Author : Shaza Darwish
Publisher : Unknown
Release : 2019
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download Mechanochemical Synthesis of Cocrystals and Metal Organic Materials book written by Shaza Darwish, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

Organic Mechanochemistry and Its Practical Applications

Organic Mechanochemistry and Its Practical Applications Book
Author : Zory Vlad Todres
Publisher : CRC Press
Release : 2006-03-06
ISBN : 142000588X
Language : En, Es, Fr & De

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Book Description :

Organic Mechanochemistry and Its Practical Applications gathers physical and organic chemistry-based molecular principles, evolving interpretations of scientific data, and real world applications to demonstrate the synthetic advantages of mechanically initiated organic reactions. This book considers transformations of organic substances upon

Eco friendly Synthesis of Fine Chemicals

Eco friendly Synthesis of Fine Chemicals Book
Author : Roberto Ballini
Publisher : Royal Society of Chemistry
Release : 2009
ISBN : 1847559085
Language : En, Es, Fr & De

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Book Description :

The 20th century has seen a phenomenal growth in the global economy and continuous improvement in the standard of living in the industrialized countries. Sustainable development has become an ideal target in recent years and in the early 1990s the concept of "Green chemistry" was launched in the USA as a new paradigm, and since 1993 it has been promoted by the National Science Foundation (NSF) and the Environmental Protection Agency (EPA). The success of the pharmaceutical industry is, in large part, due to the towering achievement of organic chemistry, a mature science which emerged as a distinct discipline well over 150 years ago, however this has been both a blessing and a curse. Many of our most reliable strategies for assembling target molecules employ reactions which are fifty to one hundred years old and are often named in honour of their discoverers. During these early years, the chronic toxicological properties of chemicals were often completely unknown and many unwittingly became indispensable tools of the trade. Early pioneers in green chemistry included Trost (who developed the atom economy principle) and Sheldon (who developed the E-Factor). These measures were introduced to encourage the use of more sustainable chemistry and provide some benchmarking data to encourage scientists to aspire to more benign synthesis. Green chemistry is essentially the design of chemical processes and procedures that reduce or eliminate the use, or the generation, of hazardous substances. Green chemistry is a growing area of research and an increasing number of researchers are now involved in this field. The number of publications has dramatically increased and new recognition of advances made is necessary with respect to other research areas. The synthesis of "Fine Chemicals" represents one of the main goals in organic synthesis and this new book extensively examines the main processes and procedures for their preparation under eco-friendly conditions. The book is a collection of selected research topics delivered by scientists involved in some of the more prominent fields of green chemistry. It is devoted to the synthesis of fine chemicals by the use of alternative eco-friendly solvents (ionic liquids, polyethylene glycol, water, etc.), supported organic catalysis, microwave irradiation or high pressure as contributors to more efficient processes, photochemistry as a green procedure and solvent-free processes. Each chapter gives an introduction to the various methods or procedures and their contribution to green chemistry and a variety of the most representative examples of the eco-friendly synthesis of fine chemicals are reported and discussed. In addition, there is a chapter dedicated to the application of simple reaction to the synthesis of complex molecules.The chapters are all written by authors who are experts in their field and are exhaustively referenced and the book will be invaluable for researchers and industrialists as well as academia.

Environmental Mechanochemistry

Environmental Mechanochemistry Book
Author : Matej Baláž
Publisher : Springer
Release : 2021-07-28
ISBN : 9783030752231
Language : En, Es, Fr & De

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Book Description :

This book provides a comprehensive overview on mechanochemistry including its history, high-energy ball milling process, equipment used and fundamentals behind the observed scientific phenomena. It also shows that mechanochemistry is highly applicable in the field of waste treatment. The text reviews 1017 studies utilizing mostly high-energy ball milling for the treatment of various types of consumer, technogenic and agricultural waste. The text is divided into chapters based on individual waste types. The book presents an Appendix compiling all studies arranged according to the application that the recycled waste is meant for. In this way, readers from both academia and companies interested either in the treatment of a particular waste, or particular application might easily locate sections of interest.

Mechanochemical Synthesis of Metal organic Frameworks

Mechanochemical Synthesis of Metal organic Frameworks Book
Author : Yuancheng Zhang
Publisher : Unknown
Release : 2017
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download Mechanochemical Synthesis of Metal organic Frameworks book written by Yuancheng Zhang, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

High Energy Ball Milling

High Energy Ball Milling Book
Author : Małgorzata Sopicka-Lizer
Publisher : Elsevier
Release : 2010-05-24
ISBN : 1845699440
Language : En, Es, Fr & De

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Book Description :

Mechanochemical processing is a novel and cost effective method of producing a wide range of nanopowders. It involves the use of a high energy ball mill to initiate chemical reactions and structural changes. High energy ball milling: Mechanochemical processing of nanopowders reviews the latest techniques in mechanochemistry and how they can be applied to the synthesis and processing of various high-tech materials. Part one discusses the basic science of mechanochemistry with chapters on such topics as the mechanism and kinetics of mechanochemical processes, kinetic behaviour in mechanochemically-induced structural and chemical transformations and materials design through mechanochemical processing. Part two reviews mechanochemical treatment of different materials including synthesis of complex ceramic oxides, production of intermetallic compound powders, synthesis of organic compounds, synthesis of metallic-ceramic composite powders and activation of covalent bond-based materials. Part three covers mechanochemical processes in metal powder systems and other applications with coverage of topics such as plating and surface modification using ultrasonic vibrations, activated powders as precursors for spark plasma sintering, titanium dioxide photocatalyst synthesis by mechanochemical doping and synthesis of materials for lithium-ion batteries. With its distinguished editor and international team of contributors, High energy ball milling: Mechanochemical processing of nanopowders is a standard reference for all those involved in the production of ceramic and metallic components using sintering and other powder metallurgy techniques to produce net shape components. Examines the latest techniques in mechanochemistry and how they can be applied to the synthesis and processing of various high-tech materials Discusses the basic science of mechanochemistry including kinetic behaviour, processes and mechanisms and materials design through mechanochemical processing Reviews mechanochemical treatment of different materials including synthesis of ceramic oxides, organic compounds and metallic-ceramic composite powders

Mechanochemistry

Mechanochemistry Book
Author : Royal Society Of Chemistry
Publisher : Unknown
Release : 2014-11-25
ISBN : 9781782621706
Language : En, Es, Fr & De

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Book Description :

The growing interest in mechanochemical processes has in the past decade provided exciting developments in the areas of supramolecular, pharmaceutical, materials and organic chemistry and catalysis.

Mechanochemical Synthesis of Paramagnetic Metal organic Materials

Mechanochemical Synthesis of Paramagnetic Metal organic Materials Book
Author : Martin Glavinovic
Publisher : Unknown
Release : 2016
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

"Metal-organic complexes and coordination polymers have emerged as promising modern materials for a variety of applications. While there have been brilliant innovations in their architectural and functional designs, the underlying synthetic methodologies have undergone little fundamental change. Today metal-organic complexes are synthesized through a combination of acid-base and ligand exchange transformations in solution involving metal salts. This synthetic pathway, which is highly dependant on the use of organic solvents, elevated temperatures or pressures, requires the use of strong bases, or the production of corrosive mineral acids as by-products. This thesis describes a novel methodology for the solvent- and waste-free mechanochemical synthesis of metal-organic materials, directly from low-valent metals and metal oxides. The synthetic strategy couples the oxidative potential of o-quinones with coordination-driven self-assembly, generating paramagnetic metal-semiquinonate and metal-catecholate units. These can then be subsequently, or in a one-pot process, patterned into mono-, di- and trinuclear complexes and coordination polymers by the addition of designed amine ligand additives with specific geometry and stoichiometry. The mechanochemical oxidative assembly is enabled by the presence of a sub-stoichiometric biphasic liquid additive, with small changes in composition some times resulting in excellent selectivity between discrete and polymeric self-assembled architectures by the inclusion of solvate guests. While the majority of the characterized structures are zinc bis-semiquinonate complexes, reactivity has been shown with a range of metals including copper, cobalt, manganese and germanium generating both paramagnetic and diamagnetic materials. Keywords: metal organic materials, mechanochemistry, solid-state chemistry, green chemistry, dioxolenes, oxidative self-assembly, paramagnetic materials" --

Mechanochemical Synthesis of Composite Materials

Mechanochemical Synthesis of Composite Materials Book
Author : Z. A. Mansurov,Nina Nikolaevna Mofa,Tlek Aitmukhanovich Ketegenov,Bakhtiyar Seisembekovich Sadykov
Publisher : Unknown
Release : 2021-08
ISBN : 9789814800884
Language : En, Es, Fr & De

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Book Description :

Mechanochemical treatment is one of the modern promising directions of the chemical and technological processes of obtaining a new substance as a result of the transformation of mechanical energy into the chemical and physical processes of system restructuring. This book presents years of research on the mechanochemical synthesis of composite systems, consisting of inorganic and organic components, obtained by the scientific team of the Institute of Combustion Problems. The book contains, first of all, general ideas about the mechanochemical process and the phenomena accompanying it. The main provisions of structural rearrangement and modification of the surface of dispersible particles are considered, as well as thermodynamics of mechanochemical treatment of materials. Then, using the example of a number of natural minerals, it is shown how mechanochemical treatment can radically change their structure and properties, using various organic compounds as modifiers. Particular attention is paid to the use of ultrasonic treatment, as a kind of mechanical action in a liquid medium on a solid.

Catalyst free Organic Synthesis

Catalyst free Organic Synthesis Book
Author : Goutam Brahmachari
Publisher : Royal Society of Chemistry
Release : 2017-11-06
ISBN : 1782624120
Language : En, Es, Fr & De

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Book Description :

Download Catalyst free Organic Synthesis book written by Goutam Brahmachari, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

High Pressure Organic Synthesis

High Pressure Organic Synthesis Book
Author : Davor Margetic
Publisher : Walter de Gruyter GmbH & Co KG
Release : 2019-07-08
ISBN : 3110556847
Language : En, Es, Fr & De

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Book Description :

High pressure chemistry is a widely used methodology in organic synthesis which helps to increase the rate and to improve the efficiency of chemical processes. The current publication outlines the impact of pressure on many types of chemical reactions important from synthetic point of view and gives practical considerations how to plan and perform synthetic experiments under high pressure in the lab.

Advances in Physical Organic Chemistry

Advances in Physical Organic Chemistry Book
Author : Ian Williams,Nick Williams
Publisher : Academic Press
Release : 2018-11-15
ISBN : 0128155396
Language : En, Es, Fr & De

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Book Description :

Advances in Physical Organic Chemistry, Volume 52 in the series, is the definitive resource for authoritative reviews of work in physical organic chemistry. It aims to provide a valuable source of information that is ideal not only for physical organic chemists applying their expertise to both novel and traditional problems, but also for non-specialists across diverse areas who identify a physical organic component in their approach to research. Its hallmark is a quantitative, molecular level understanding of phenomena across a diverse range of disciplines. Reviews the application of quantitative and mathematical methods to help readers understand chemical problems Provides the chemical community with authoritative and critical assessments of the many aspects of physical organic chemistry Covers organic, organometallic, bioorganic, enzymes and materials topics Presents the only regularly published resource for reviews in physical organic chemistry Written by authoritative experts who cover a wide range of topics that require a quantitative, molecular-level understanding of phenomena across a diverse range of disciplines

Organic Sonochemistry

Organic Sonochemistry Book
Author : Jean-Marc Lévêque,Giancarlo Cravotto,François Delattre,Pedro Cintas
Publisher : Springer
Release : 2018-10-11
ISBN : 331998554X
Language : En, Es, Fr & De

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Book Description :

This book provides informative, useful, and stimulating reading on the topic of organic sonochemistry – the core of ultrasound-based applications. Given the increasing interest in new and improved technologies, allied to their green and sustainable character (not always a valid premise), there is a great attraction for organic chemists to apply these protocols in synthesis and process chemistry. Unfortunately, as with other enabling technologies, many researchers new to the field have received a simple and dishonest message: just switch on! Therefore a significant portion of sonochemical syntheses lack reproducibility (surprisingly cavitation control and/or ultrasonic parameters are omitted) and the actual role of sonication remains uncertain. While this book does not provide a detailed description of fundamentals, the introductory remarks highlight the importance of cavitational effects and their experimental control. It presents a number of concepts of sonochemical reactivity and empirical rules with pertinent examples, often from classical and recent literature. It then focuses on scenarios of current interest where organic chemistry, and synthesis in particular, may benefit from sonication in terms of both chemical and mechanical activation. The “sustainable corner” of this field is largely exemplified through concepts like atom economy, renewable sources, wasteless syntheses, and benign solvents as reaction media. This book is useful for both researchers and graduate students, especially those familiar with the field of sonochemistry and applications of ultrasound in general. However, it is also of interest to a broader audience as it discusses the fundamentals, techniques, and experimental skills necessary for scientists wishing to initiate the use of ultrasound in their domain of expertise.