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Capillary Electromigration Separation Methods

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Capillary Electromigration Separation Methods

Capillary Electromigration Separation Methods Book
Author : Colin F. Poole
Publisher : Elsevier
Release : 2018-04-13
ISBN : 0128096144
Language : En, Es, Fr & De

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Book Description :

Capillary Electromigration Separation Methods is a thorough, encompassing reference that not only defines the concept of contemporary practice, but also demonstrates its implementation in laboratory science. Chapters are authored by recognized experts in the field, ensuring that the content reflects the latest developments in research. Thorough, comprehensive coverage makes this the ideal reference for project planning, and extensive selected referencing facilitates identification of key information. The book defines the concept of contemporary practice in capillary electromigration separation methods, also discussing its applications in small mass ions, stereoisomers, and proteins. Edited and authored by world-leading capillary electrophoresis experts Presents comprehensive coverage on the subject Includes extensive referencing that facilitates the identification of key research developments Provides more than 50 figures and tables that aid in the retention of key concepts

On line and Off line Enrichment Techniques Combined with Capillary Electromigration Separation Methods in the Analysis of Highly Hydrophilic Analytes in Biological and Environmental Samples

On line and Off line Enrichment Techniques Combined with Capillary Electromigration Separation Methods in the Analysis of Highly Hydrophilic Analytes in Biological and Environmental Samples Book
Author : Azza Hesham Rageh
Publisher : Unknown
Release : 2015
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download On line and Off line Enrichment Techniques Combined with Capillary Electromigration Separation Methods in the Analysis of Highly Hydrophilic Analytes in Biological and Environmental Samples book written by Azza Hesham Rageh, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

Analytical Separation Science 5 Volume Set

Analytical Separation Science  5 Volume Set Book
Author : Jared Anderson,Alain Berthod,Veronica Pino,Apryll M. Stalcup
Publisher : Wiley-VCH
Release : 2016-02-29
ISBN : 9783527333745
Language : En, Es, Fr & De

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Book Description :

Leading the way for analytical chemists developing new techniques. This new comprehensive 5 volume set on separation science provides a much needed research-level text for both academic users and researchers who are working with and developing the most current methods, as well as serving as a valuable resource for graduate and post-graduate students. Comprising of five topical volumes it provides a comprehensive overview of the subject, highlighting aspects that will drive research in this field in the years to come. Volume 1: Liquid Chromatography Volume 2: Special Liquid Chromatography Modes and Capillary Electromigration Techniques Volume 3: Gas, Supercritical and Chiral Chromatography Volume 4: Chromatographic and Related Techniques Volume 5: Sample Treatment, Method Validation, and Applications Key Features: - Comprises over 2,100 pages in 5 volumes – available in print and online - Edited by an international editorial team which has both prominent and experienced senior researchers as well as young and dynamic rising stars - Individual chapters are labeled as either introductory or advanced, in order to guide readers in finding the content at the appropriate level - Fully indexed with cross referencing within and between all 5 volumes

Use of non specific and specific interactions in the analysis of testosterone and related compounds by capillary electromigration techniques

Use of non specific and specific interactions in the analysis of testosterone and related compounds by capillary electromigration techniques Book
Author : Lotta K. Amundsen
Publisher : Unknown
Release : 2008
ISBN : 9789513870850
Language : En, Es, Fr & De

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Book Description :

Determination of testosterone and related compounds in body fluids is of utmost importance in doping control and the diagnosis of many diseases. Capillary electromigration techniques are a relatively new approach for steroid research. Owing to their electrical neutrality, however, separation of steroids by capillary electromigration techniques requires the use of charged electrolyte additives that interact with the steroids either specifically or non-specifically. The analysis of testosterone and related steroids by non-specific micellar electrokinetic chromatography (MEKC) was investigated in this study. The partial filling (PF) technique was employed, being suitable for detection by both ultraviolet spectrophotometry (UV) and electrospray ionization mass spectrometry (ESI-MS). Efficient, quantitative PF-MEKC-UV methods for steroid standards were developed through the use of optimized pseudostationary phases comprising surfactants and cyclodextrins. PF-MEKC-UV proved to be a more sensitive, efficient and repeatable method for the steroids than PF-MEKC-ESI-MS. We discovered that in PF-MEKC analyses of electrically neutral steroids, ESI-MS interfacing sets significant limitations not only on the chemistry affecting the ionization and detection processes, but also on the separation. The new PF-MEKC-UV method was successfully employed in the determination of testosterone in male urine samples after microscale immunoaffinity solid-phase extraction (IA-SPE). The IA-SPE method, relying on specific interactions between testosterone and a recombinant anti-testosterone Fab fragment, is the first such method described for testosterone. Finally, new data for interactions between steroids and human and bovine serum albumins were obtained through the use of affinity capillary electrophoresis. A new algorithm for the calculation of association constants between proteins and neutral ligands is introduced.

Quality Control in Pharmaceutical Analysis

Quality Control in Pharmaceutical Analysis Book
Author : Z. Deyl
Publisher : Elsevier Science Limited
Release : 1997-01-01
ISBN : 9780444828767
Language : En, Es, Fr & De

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Book Description :

It is difficult, if not impossible, to visualize pharmaceutical industry processes without appropriate analytical control, of which chromatographic and, more recently, capillary electromigration techniques constitute a considerable proportion. Problems such as deciding which separation technique will be the best, whether a chromatographic or an electrokinetically driven method is preferred, calibration procedures and method validation, identification of impurities by on-line hyphenation with techniques based on physicochemical principles other than chromatography and electrophoresis and assaying of basic physicochemical properties are all to be solved by the analytical chemist. Unintended errors can occur quite frequently. This volume covers all the above outlined areas, emphasizing those which the authors know from pharmaceutical research to cause problems in practice. The basic guidelines have been summarized along with the necessary theoretical background to help analysts select and apply modern chromatographic and electrokinetic methods of analysis in drug production and quality control and help them solve their particular problems.

Special Issue 16th International Symposium on Separation Sciences New Advancements in Chromatography and Capillary Electromigration Techniques

Special Issue  16th International Symposium on Separation Sciences  New Advancements in Chromatography and Capillary Electromigration Techniques Book
Author : Danilo Corradini
Publisher : Unknown
Release : 2011
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download Special Issue 16th International Symposium on Separation Sciences New Advancements in Chromatography and Capillary Electromigration Techniques book written by Danilo Corradini, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

The Essence of Chromatography

The Essence of Chromatography Book
Author : C. F. Poole
Publisher : Elsevier
Release : 2003
ISBN : 9780444501998
Language : En, Es, Fr & De

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Book Description :

The Essence of Chromatography presents a comprehensive survey of modern chromatography and is intended as a suitable text for graduate level courses in the separation sciences and as a self-study guide for professional chromatographers wishing to refresh their background in this rapidly expanding field. This title is an effective replacement for Chromatography Today, written by the same author with Salwa K. Poole, which is considered to be one of the definitive chromatographic texts of the last decade. Its format is modular, with extensive cross-references to permit rapid location of related material using different separation concepts. Important features are extensive tabulation of essential data for performing separations and an extensive bibliography to the most recent literature. · Comprehensive and authoritative coverage of chromatographic techniques · Contains extensive coverage of recent literature on this subject · Ideal text for graduates and suitable for professional chromatographers

16th International Symposium on Separation Sciences

16th International Symposium on Separation Sciences Book
Author : Danilo Corradini
Publisher : Unknown
Release : 2011
ISBN : 0987650XXX
Language : En, Es, Fr & De

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Book Description :

Download 16th International Symposium on Separation Sciences book written by Danilo Corradini, available in PDF, EPUB, and Kindle, or read full book online anywhere and anytime. Compatible with any devices.

Chiral Separation Methods for Pharmaceutical and Biotechnological Products

Chiral Separation Methods for Pharmaceutical and Biotechnological Products Book
Author : Satinder Ahuja
Publisher : John Wiley & Sons
Release : 2011-03-31
ISBN : 9781118097755
Language : En, Es, Fr & De

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Book Description :

Discusses chiral separations and offers guidance for selectingthe optimum method for desired results Chiral separations represent the most intriguing and, by somemeasures, most difficultseparations of chemical compounds. Thisbook provides researchers and students an under-standing of chiralseparations and offers a convenient route to selecting the bestseparation method, saving considerable time and cost in productdevelopment. Considering chiral separations in the biotechnological andpharmaceutical industries, as well as for food applications, Dr.Ahuja provides insights into a broad range of topics. Opening witha broad overview of chiral separations, regulatory considerationsin drug product development, and basic issues in methoddevelopment, the book: Covers a variety of modern methods such as gas chromatography,high performance liquid chromatography, supercritical fluidchromatography, and capillary electrophoresis Deals with the impact of chirality on the biological activity ofsmall and large molecules Provides detailed information on useful chiral stationary phases(CSPs) for HPLC Includes handy information on selection of an appropriate CSP,including mechanistic studies Offers strategies for fast method development with HPLC, SFC,and CE Discusses preparatory methods utilized in the pharmaceuticalindustry With in-depth discussions of the current state of the field aswell as suggestions to assist future developments, ChiralSeparation Methods for Pharmaceutical and BiotechnologicalProducts is an essential text for laboratory investigators,managers, and regulators who are involved in chiral separations inthe pharmaceutical industry, as well as students preparing forcareers in these fields.

Encyclopedia of Analytical Science

Encyclopedia of Analytical Science Book
Author : Anonim
Publisher : Elsevier
Release : 2019-04-02
ISBN : 008101984X
Language : En, Es, Fr & De

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Book Description :

The third edition of the Encyclopedia of Analytical Science is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher

Chiral Recognition in Separation Methods

Chiral Recognition in Separation Methods Book
Author : Alain Berthod
Publisher : Springer Science & Business Media
Release : 2010-06-16
ISBN : 3642124453
Language : En, Es, Fr & De

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Book Description :

What drives a scientist to edit a book on a speci c scienti c subject such as chiral mechanisms in separation methods? Until December 2005, the journal Analytical Chemistry of the American Chemical Society (Washington, DC) had an A-page section that was dedicated to simple and clear presentations of the most recent te- niques or the state of the art in a particular eld or topic. The “A-page” section was prepared for a broad audience of chemists including industrial professionals, s- dents as well as academics looking for information outside their eld of expertise. 1 Daniel W. Armstrong, one of the editors of this journal and a twenty-year+ long friend, invited me to present my view on chiral recognition mechanisms in a simple and clear way in an “A-page” article. In 2006, the “A-page” section was maintained as the rst articles at the beginning of each rst bi-monthly issue but the pagination was no longer page distinguished from the regular research articles published by the journal. During the time between the invitation and the submission, the A-page section was integrated into the rest of the journal and the article appeared as (2006) Anal Chem (78):2093–2099.

Electromigration Techniques

Electromigration Techniques Book
Author : Boguslaw Buszewski,Ewelina Dziubakiewicz,Michal Szumski
Publisher : Springer Science & Business Media
Release : 2013-04-23
ISBN : 3642350437
Language : En, Es, Fr & De

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Book Description :

The book provides the broad knowledge on electromigration techniques including: theory of CE, description of instrumentation, theory and practice in micellar electrokinetic chromatography, isotachophoresis, capillary isoelectric focusing, capillary and planar electrochromatography (including description of instrumentation and packed and monolithic column preparation), 2D-gel electrophoresis (including sample preparation) and lab-on-a-chip systems. The book also provides the most recent examples of applications including food, environmental, pharmaceutical analysis as well as proteomics.

Advanced Chromatographic and Electromigration Methods in BioSciences

Advanced Chromatographic and Electromigration Methods in BioSciences Book
Author : I. Mikšík,F. Tagliaro,E. Tesarová,Z. Deyl
Publisher : Elsevier
Release : 1998-09-28
ISBN : 9780080858685
Language : En, Es, Fr & De

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Book Description :

This book deals with chromatographic and electrophoretic methods applied for the separation (quantitation and identification) of biologically relevant compounds. It is assumed that the potential reader is familiar with the basics of chromatographic and electromigration methods. Individual separation modes are dealt with to an extent which follows their applicability for biomedical purposes: liquid chromatography and electromigration methods are therefore highlighted. Each chapter is completed with a list of recent literature covering the 1987-1997 period, which can be used for further guidance of the reader in his/her own field. The chapters have been written by specialists in a particular area and with an emphasis on applications to the biomedical field. This implies that theoretical and instrumental aspects are kept to a minimum which allows the reader to understand the text. Considerable attention is paid to method selection, detection and derivatization procedures and troubleshooting. The majority of examples given represent the analyses of typical naturally-occurring mixtures. Adequate attention is paid to the role of the biological matrix and sample pretreatment, and special attention is given to forensic, toxicological and clinical applications. The book is completed with an extensive Index of Compounds Separated.

Handbook of HPLC

Handbook of HPLC Book
Author : Danilo Corradini
Publisher : CRC Press
Release : 2016-04-19
ISBN : 1420016946
Language : En, Es, Fr & De

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Book Description :

High performance liquid chromatography (HPLC) is one of the most widespread analytical and preparative scale separation techniques used for both scientific investigations and industrial and biomedical analysis. Now in its second edition, this revised and updated version of the Handbook of HPLC examines the new advances made in this field since the

Analytical Separation Science

Analytical Separation Science Book
Author : Jared Anderson,Alain Berthod,Veronica Pino,Apryll M. Stalcup
Publisher : John Wiley & Sons
Release : 2016-02-08
ISBN : 3527333746
Language : En, Es, Fr & De

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Book Description :

Leading the way for analytical chemists developing new techniques. Introductory Price Available! Order your print copy before 30th April 2016 and save! £650 / $1,075 / €799 List price thereafter: £735 / $1,210 / €899 This new comprehensive 5 volume set on separation science provides a much needed research-level text for both academic users and researchers who are working with and developing the most current methods, as well as serving as a valuable resource for graduate and post-graduate students. Comprising of five topical volumes it provides a comprehensive overview of the subject, highlighting aspects that will drive research in this field in the years to come. Volume 1: Liquid Chromatography Volume 2: Special Liquid Chromatography Modes and Capillary Electromigration Techniques Volume 3: Gas, Supercritical and Chiral Chromatography Volume 4: Chromatographic and Related Techniques Volume 5: Sample Treatment, Method Validation, and Applications Key Features: - Comprises over 2,100 pages in 5 volumes – available in print and online - Edited by an international editorial team which has both prominent and experienced senior researchers as well as young and dynamic rising stars - Individual chapters are labeled as either introductory or advanced, in order to guide readers in finding the content at the appropriate level - Fully indexed with cross referencing within and between all 5 volumes

Capillary Gel Electrophoresis

Capillary Gel Electrophoresis Book
Author : Andras Guttman,László Hajba
Publisher : Newnes
Release : 2021-12-03
ISBN : 0080931359
Language : En, Es, Fr & De

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Book Description :

Capillary Gel Electrophoresis and Related Microseparation Techniques covers all theoretical and practical aspects of capillary gel electrophoresis. It also provides an excellent overview of the key application areas of nucleic acid, protein and complex carbohydrate analysis, affinity-based methodologies, micropreparative aspects and related microseparation methods. It not only gives readers a better understanding of how to utilize this technology, but also provides insights into how to determine which method will provide the best technical solutions to particular problems. This book can also serve as a textbook for undergraduate and graduate courses in analytical chemistry, analytical biochemistry, molecular biology and biotechnology courses. Covers all theoretical and practical aspects of capillary gel electrophoresis Excellent overview of the key applications of nucleic acid, protein and complex carbohydrate analysis, affinity-based methodologies, micropreparative aspects and related microseparation methods Teaches readers how to use the technology and select methods that are ideal for fundamental problems Can serve as a textbook for undergraduate and graduate courses in analytical chemistry, analytical biochemistry, molecular biology and biotechnology courses

Electrokinetic Chromatography

Electrokinetic Chromatography Book
Author : Ute Pyell
Publisher : John Wiley & Sons
Release : 2007-01-11
ISBN : 0470871032
Language : En, Es, Fr & De

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Book Description :

This book offers a thorough theoretical description of the method, an overview on the current status of the various forms of electrokinetic capillary chromatography, plus a look forward into future developments. Focuses on the technique of electrokinetic capillary chromatography and its applications in various areas, including pharmaceutical, industrial, environmental, and biological chemistry Features invaluable information put together from experienced researchers in the area First book to discuss this technique in detail Covers a topic that is part of the exploding field of hyphenated techniques Selected international contributors working in research in this area

Chiral Separations by Capillary Electrophoresis

Chiral Separations by Capillary Electrophoresis Book
Author : Ann Van Eeckhaut,Yvette Michotte
Publisher : CRC Press
Release : 2009-11-11
ISBN : 9781420069341
Language : En, Es, Fr & De

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Book Description :

Covers the Fundamentals of Chiral Separation, Available Chiral Selectors, and Numerous Applications of Chiral Separation by Capillary Electrophoresis Since the 1980s, modern analytical tools have enabled capillary electrophoresis to become a standard part of the chemist’s toolkit. With contributions from international experts, Chiral Separations by Capillary Electrophoresis provides a general overview of the principles of chiral separation by capillary electrophoresis and the different chiral selectors available. The book discusses the most important as well as several new chiral selectors used in capillary electrophoresis. It reviews recent pharmaceutical and biomedical applications and explores novel techniques, such as capillary electrophoresis coupled to mass spectrometry and microchip technology. The book also examines the quantitative aspects of capillary electrophoresis, the possibilities of capillary electrochromatography, and the various chiral columns available. Capillary electrophoresis has proven to be an effective tool for chiral separation. This book explains how this technique can be used in the separation of molecules, offering insight into both existing and emerging applications.

Principles and Practice of Modern Chromatographic Methods

Principles and Practice of Modern Chromatographic Methods Book
Author : Kevin Robards,Danielle Ryan
Publisher : Academic Press
Release : 2021-05-01
ISBN : 012822097X
Language : En, Es, Fr & De

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Book Description :

Principles and Practice of Modern Chromatographic Methods, Second Edition takes a comprehensive, unified approach in its presentation of chromatographic techniques. Like the first edition, the book provides a scientifically rigid, but easy-to-follow presentation of chromatography concepts that begins with the purpose and intent of chromatographic theory - the “what and why that are left out of other books attempting to cover these principles. This fully revised second edition brings the content up-to-date, covering recent developments in several new sections and an additional chapter on composite methods. New topics include sample profiling, sample preparation, sustainable green chemistry, 2D chromatography, miniaturization/nano-LC, HILIC, and more. Contains thorough chapters that begin with an updated schematic overview and a visual representation of the content Avoids the obfuscation of different terminologies and classification systems that are prevalent in the area, such as the relationship between liquid chromatography and column chromatography Provides integrated and comprehensive topic coverage based on chromatographic bibliometrics and survey reports on the relative usage of chromatographic techniques